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Lecturer(s)
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Fryčák Petr, doc. RNDr. Ph.D.
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Pauk Volodymyr, Mgr. Ph.D.
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Lemr Karel, prof. RNDr. Ph.D.
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Skopalová Jana, doc. RNDr. Ph.D.
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Borovcová Lucie, Mgr. Ph.D.
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Course content
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Introduction to instrumental analytical methods. Selected optical methods - spectral (emission and absorption), non-spectral (refractometry, polarimetry). Electromagnetic spectrum and basic laws of absorption and emission of irradiation. Introduction to mass spectrometry. Selected electroanalytical methods (potentiometry, conductometry, coulometry, polarography and modern voltammetric methods). Selected separation methods (separation, chromatography, electromigration methods). Seminar: practicing and deepening of mentioned topics. Composition and preparation of solution. Gravimetric and titrimetric stoichiometry. Acid-base, complexometric, oxidation-reduction, and precipitation equilibria, calculation of corresponding quantities, calculation of titration curves and concentration of compounds in different points of titration. Examples from instrumental methods.
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Learning activities and teaching methods
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Lecture, Dialogic Lecture (Discussion, Dialog, Brainstorming)
- Attendace
- 52 hours per semester
- Homework for Teaching
- 26 hours per semester
- Preparation for the Course Credit
- 12 hours per semester
- Preparation for the Exam
- 30 hours per semester
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Learning outcomes
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To provide students with basic knowledge of selected instrumental methods used in analytical chemistry.
To describe main approaches applied in instrumental analytical chemistry, to suggest suitable analytical procedures for a given analytical task. To be familiar with data that can be obtained by studied instrumental methods.
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Prerequisites
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The knowledge of basics of general, organic, anorganic, physical and analytical chemistry is recommended.
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Assessment methods and criteria
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Written exam
Student has to pass the written test, to reach 60% points. Knowledge of topics of the subject ACH/AC1 is presupposed. Grasp of practical laboratory tasks (the subject ACH/ACC) is presupposed too. The attendance in seminar is obligatory.
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Recommended literature
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Barek J., Opekar F., Štulík K. (2005). Elektroanalytická chemie. Karolinum Praha.
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de Hoffmann E., Stroobant V. (2007). Mass Spectoskopy, Principles and Applications. John Wiley and sons.
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Harvey D. (2000). Modern Analytical Chemistry. McGraw-Hill, New York.
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Christian G.D., Dasqupta P.K., Schug K.A. (2014). Analytical chemistry 7th. ed.. Wiley Hoboken.
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I. Wilson, C. Poole, M. Cooke. (2000). Encyclopedia of separation science. Academic Press, San Diego, London, Boston, New York, Sydney, Tokyo, Toronto.
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Kotouček, M. Příklady z analytické chemie, UP Olomouc 1982;.
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Štulík K., Ševčík J., Pacáková V., Jelínek I., Coufal P., Bosáková Z. (2004). Analytické separační metody. Karolinum Praha.
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Wang, J. (2006). Analytical electrochemistry. Wiley-VCH, NY.
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Záruba K. a kolektiv. (2016). Analytická chemie (1.díl). VŠCHT Praha.
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