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Lecturer(s)
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Berka Karel, doc. RNDr. Ph.D.
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Štefková Barbora, RNDr.
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Ranc Václav, doc. RNDr. Ph.D.
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Prucek Robert, doc. RNDr. Ph.D.
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Course content
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Mass spectroscopy (MS) - principle and application; experimental setup; types of ionization; mass analyzers; MS detectors; MS spectrum; molecular ion and its fragmentation; effect of natural isotopes Nuclear magnetic resonance (NMR) - principle and exploitation; magnetic properties of atoms and molecules; relaxation; chemical shifts and spin-spin splitting; instrumentation in NMR; monitoring of chemical exchange due to NMR Electron paramagnetic resonance (EPR) - principle and exploitation; experimental setup; spin-orbital and spin-spin interactions in EPR Roentgen spectrometry - theoretical basics; application of primary Roentgen radiation; application of secondary Roentgen radiation (Roentgen fluorescence spectrometry); exploitation of X-ray absorption (Roentgen absorption spectrometry); X-ray diffraction (crystals, powders, liquid crystals) Basics of electron spectroscopy - principles and applications: photoelectron spectroscopy (XPS, UPS); Auger electron spectroscopy (X-AES, E-AES) Basics of X-ray fluorescence analysis (XRF) Basics of laser spectrometry - principle of laser; significant types and examples of lasers; laser spectroscopy - linear, nonlinear and special methods Neutron diffraction and neutron activation analysis (NAA) - principles; experimental setup; applications
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Learning activities and teaching methods
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Monologic Lecture(Interpretation, Training)
- Preparation for the Exam
- 48 hours per semester
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Learning outcomes
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The lecture is aimed to teach basics of particular spectroscopic methods mentioned bellow.
Knowledge of basics of methods.
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Prerequisites
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unspecified
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Assessment methods and criteria
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Oral exam
Participation on lecture is not obligatory but is highly recommanded.
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Recommended literature
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Boudroux E. A., Mulay L. N. (1976). Theory and applications of molecular paramagnetism. Wiley&Sons N.Y.
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Ed. C. Giacivazzo. (1992). Fundamentals of Crystallography. Oxford University Press, IUCr, ().
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Kalous, V. (1987). Metody chemického výzkumu. SNTL, Praha.
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Lindon, J.C., Tranter, G.E., Holmes, J.L. Encyclopiedia of spectroscopy and spectrometry II..
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Moore J.H., Spencer N.D. Encyclopedia of chemical physics and physical chemistry.
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Prosser,V. a kol. (1989). Experimentální metody biofyziky. Academia Praha.
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