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Lecturer(s)
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Bužková Aneta, Mgr.
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Berka Karel, prof. RNDr. Ph.D.
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Prucek Robert, doc. RNDr. Ph.D.
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Course content
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1. Introduction, basic concepts, basic principles, classification. 2. UV-Vis absorption spectroscopy. Fundamentals of instrumentation, basic principles. Radiation sources. 3. Infrared spectroscopy. FTIR spectroscopy. Fundamentals of instrumentation, basic principles, vibrational-rotational spectra of substances and their interpretation. Examples of applications. 4. Raman spectroscopy - fundamentals, instrumentation, surface-enhanced Raman scattering (SERS) spectroscopy. Fundamentals and examples of possible uses. 5. Fluorescence, phosphorescence, luminescence. Fundamentals. Possible uses. 6. Atomic absorption spectroscopy (AAS), atomic emission spectroscopy (AES), fundamentals, possible uses. ICP spectroscopy. 7. X-ray powder diffraction, electron and neutron diffraction. Generation and detection of X-ray radiation. Basic principles (Bragg's law), particle size measurement using low-angle X-ray scattering (SAXS). 8. Methods based on the emission/absorption of electrons/X-rays induced by the action of photons or particles. X-ray fluorescence spectroscopy (XRF). Basic principles (Moseley's law, Rayleigh and Compton scattering, secondary fluorescence). 9. Photoelectron spectroscopy (UPS, XPS/ESCA), Auger electron spectroscopy, X-ray absorption spectroscopy (XAS - EXAFS, XANES). 10. Mass spectrometry, interpretation of mass spectra. 11. Mössbauer spectroscopy. Mössbauer effect, experimental observation of the Mössbauer effect, hyperfine interactions, interpretation of Mössbauer spectra, low-temperature Mössbauer spectroscopy and spectroscopy in an external magnetic field. 12. Nuclear magnetic resonance. Nuclear magnetic moment. Magnetic moment in a magnetic field. Free precession. Spin and stimulated echo. NMR spectra. Chemical shift, signal splitting, double resonance, NMR of nuclei other than protons, NMR tomography. Magnetic resonance imaging (MRI). EPR spectroscopy.
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Learning activities and teaching methods
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Monologic Lecture(Interpretation, Training)
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Learning outcomes
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Students will be introduced to a variety of analytical methods, such as: UV-Vis absorption spectroscopy. Infrared spectroscopy. FTIR spectroscopy. Raman spectroscopy - basics, instrumentation, surface-enhanced Raman scattering (SERS) spectroscopy. Fluorescence, phosphorescence, luminescence. Atomic absorption spectroscopy (AAS), atomic emission spectroscopy (AES). X-ray powder diffraction, electron and neutron diffraction. Methods based on the emission/absorption of electrons/X-rays induced by the action of photons or particles. X-ray fluorescence spectroscopy (XRF). Photoelectron spectroscopy (UPS, XPS/ESCA), Auger electron spectroscopy, X-ray absorption spectroscopy (XAS - EXAFS, XANES). Mass spectrometry, interpretation of mass spectra. Mössbauer spectroscopy. Nuclear magnetic resonance.
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Prerequisites
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unspecified
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Assessment methods and criteria
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Student performance
Students sitting the examinations should be able to discuss two chosen questions
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Recommended literature
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Dheeraj Kumar Singh, Manik Pradhan, Arnulf Materny. (2021). Modern Techniques of Spectroscopy.
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John C. Lindon. (2010). Encyclopedia of Spectroscopy and Spectrometry.
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Sam Zhang, Lin Li, Ashok Kumar. (2008). Materials Characterization Techniques.
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