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Lecturer(s)
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Bužková Aneta, Mgr.
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Berka Karel, doc. RNDr. Ph.D.
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Štefková Barbora, RNDr.
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Prucek Robert, doc. RNDr. Ph.D.
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Course content
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The practice will include the measurements of the selected samples, data processing and evaluation. Practice: 1. Size and morphological characterization of the nanoparticles via AFM method. 2. Study of thermal decomposition of the selected iron salts via TG/DTA. 3. Determination of the surface area of nanocrystalline and porous materials. 4. Measurements and evaluation of the magnetic characteristics of the selected metal oxides. 5. Measurements and evaluation of the Mössbauer spectra of the selected minerals and iron salts. 6. Measurements of size distribution of colloidal Ag via DLS method. 7. X-ray powder diffraction analysis used for the purpose of study of phase composition of the selected polycrystalline samples. 9. IR spectroscopy used for characterization of some surface modified nanoparticles - data processing, evaluation. 10. Raman spectroscopy used for characterization of some surface modified nanoparticles - data processing, evaluation.
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Learning activities and teaching methods
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Monologic Lecture(Interpretation, Training), Dialogic Lecture (Discussion, Dialog, Brainstorming), Demonstration
- Preparation for the Course Credit
- 120 hours per semester
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Learning outcomes
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The students will get acquainted with numerous techniques used for the purpose of the material and solid sample analysis.
Ability to apply and practice fundamental procedures and analyses of materials and solid samples
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Prerequisites
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unspecified
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Assessment methods and criteria
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Written exam
100% participation in the exercise; final presentation of the results of all techniques on which the measurements were made.
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Recommended literature
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http://www.upol.cz/resources/exfyz/bf/expmet1.htm ..
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E.A.BOUDROUX, L.N.MULAY. (1976). Theory and applications of molecular paramagnetism. Wiley&Sons N.Y..
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F.Březina a kol. (1988). Stereochemie a některé fyzikálně-chemické metody studia anorganických látek. Scrpt. UP Olomouc.
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F.E.MABBS, D.J.MACHIN. (1973). Magnetism and Transition Metal Complexes. Chapman and Hall, London.
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J. ROSICKÝ. (1989). Termická analýza. Praha.
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Jiří Fišer. (2002). Úvod do molekulové symetrie (Aplikace teorie grup v chemii) : Mikroskopie skenující sondou. Vydavatelství UPOlomouc.
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K. Györyová, V. Bálek. (1992). Termická analýza. Košice.
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L.Reimer. (1988). Scanning Electron Microscopy - Physics of Image Formation and Microanalysis. Springer.
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V.Prosser. (1989). Experimentální metody biofyziky. Academia Praha.
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